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莪术油冻干粉针中莪术醇的含量测定方法研究

Determination Method of Curcumol Content in Zedoary Turmeric Oil Powder and the Investigation of the Stability of Zedoary Turmeric Oil Powder

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【作者】 艾莉董英杰张乃先穆瑛俊

【Author】 AI Li1,DONG Ying-jie1,ZHANG Nai-xian1,MU Ying-jun2(1.Liaoning Institute of Pharmaceutical Industry,Shenyang 110015,Liaoning,China;2.Shenyang Wanjia Institute of Biological Technology,Shenyang 110015,Liaoning,China)

【机构】 辽宁省医药工业研究院沈阳市万嘉生物技术研究所 辽宁沈阳110015辽宁沈阳110015

【摘要】 目的:建立莪术油冻干粉针中莪术醇的含量测定方法。方法:含量测定采用GC法。结果:莪术醇与内标及其他挥发性成分分离良好,莪术醇在20.5~184.5μg/mL范围内线性关系良好,r=0.9999,平均加样回收率为100.6%,RSD为1.0%。结论:GC法能很好的分离检测莪术油冻干粉针中的莪术醇,方法简便、准确、专属性强,可用于莪术油冻干粉针的质量控制研究。

【Abstract】 Objective:To develop a new method for the determination of curcumol in Zedoary turmeric oil powder,and apply to the method to investigate the stability of Zedoary turmeric oil powder.Methods:the content of curcumol was determinationed by gas chromatography.Results:The methods can be used to determine curcumol with accuracy at a perfect line range between 20.5μg/mL and 184.5μg/mL,a recovery of 100.6%,and RSD of 1.0%.Conclusions:The present study provided a satisfactory GC method for the quantitative determination of curcumol in Zedoary turmeric oil powder,and the method seemed accurate and reliable as well as excellent reproducibility.Therefore,this method can be used as a quantitative analytical method in quality control of Zedoary turmeric oil powder.

  • 【文献出处】 辽宁中医杂志 ,Liaoning Journal of Traditional Chinese Medicine , 编辑部邮箱 ,2007年09期
  • 【分类号】R286.0
  • 【被引频次】2
  • 【下载频次】204
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