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脱氢松香酸β-萘酚酯的合成

Synthesis of dehydroabitetic acid-β-naphthol ester

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【作者】 耿哲段文贵韦瑞松岑波

【Author】 GENG Zhe,DUAN Wen-gui,WEI Rui-song,CEN Bo(College of Chemistry and Chemical Engineering,Guangxi University,Nanning,530004,China)

【机构】 广西大学化学化工学院广西大学化学化工学院 广西南宁530004广西南宁530004

【Abstract】 Dehydroabitetic acid-β-naphthol ester was prepared by O-acylation reaction of dehydroabitetic acid and β-naphthol in the presence of pyridine as catalyst.The main influence factors were studied and the optimum reaction conditions were found by orthogonal experimental design to be as follows∶ reaction temperature 100℃,reaction time 3.0h,the molar ratio of dehydroabitetic acyl chloride to pyridine 1∶1.4,the molar ratio of dehydroabitetic acyl chloride to β-naphthol 1∶1.2,the yield amounted to 78.5% with the purity of 97.62%.The target product was analyzed and characterized by IR,TLC and GC-MS methods.

【基金】 国家教育部留学回国人员科研启动基金资助项目(教外司留[2005]383号)
  • 【文献出处】 化学研究与应用 ,Chemical Research and Application , 编辑部邮箱 ,2007年01期
  • 【分类号】O621.3
  • 【被引频次】9
  • 【下载频次】280
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