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国产光栅近红外光谱仪扫描条件对检测结果的影响
Influence of Spectrometer Scanning Requirements in Homemade Grating Diffuse NIR Instrument on NIR Veracity
【摘要】 以云南优质烤烟为实验材料,在国产光栅漫反射型近红外仪器上,研究了采集间隔、开机时长、背景测量频率等扫描条件对近红外检测结果的影响。研究结果表明8,16nm的光谱数据采集间隔对近红外烤烟定量分析的影响不大,为提高采集速度确定该仪器的采集间隔为16nm;建立了包含开机时长因素在内的模型,提高模型的适应性;该仪器具有基线漂移提示功能,从而确定仪器背景采集的频率,可以降低分析误差,提高检测结果的准确度。
【Abstract】 The influence of instrument parameters, such as scan internal, length of instrument run, frequency of scan background etc, on NIR veracity was studied with a homemade grating diffuse NIR instrument using Yunnan flue-cured tobacco. Results showed that scan interval, such as 8 nm or 16 nm, had no evident influence on NIR quantitative analysis. To improve scan speed, the scan interval the authors decided to use was 16 nm. NIR model was set up which could revise the influence of the length of instrument run. This instrument can clue on baseline shift to decide the frequency of background scanning, which can deduce NIR analysis error and improve NIR veracity.
- 【文献出处】 光谱学与光谱分析 ,Spectroscopy and Spectral Analysis , 编辑部邮箱 ,2007年02期
- 【分类号】O657.33
- 【被引频次】21
- 【下载频次】283