【摘要】 以BaCl₂、TiCl₄为原料,以（NH₄）₂C₂O₄·H₂O为沉淀剂,利用微波-沉淀法制备了高纯四方相钛酸钡纳米粉体。应用XRD、TEM等对粉体的结构、形貌进行了分析。研究表明,微波-沉淀法合成粉体的时间为50 min,制备的粉体属于四方相晶体结构,粒度为30nm、粒度分布均匀,杂质含量达到电子行业工业标准。更多还原

【Abstract】 Through the microwave-precipitation process,the super-pure nanopowders barium titanate were prepared by using titanium tetrachloride and barium chloride as raw materials and （NH₄）₂C₂O₄·H₂O as the precipitant and alcohol as dispersant.The particle size,crystal phase and figure were detailed discussed using XRD and TEM.The experimental results show that the powders by the microwave- precipitation process have higher purity,finer particle （size is 30 nm）,more uniform size distribution, but the synthesization time of powders is only 50min.更多还原