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Fe2O3基纳米粉体的微乳液法制备及其气敏性

The preparation of nano Fe2O3 powder via W/O microemulsion method and its gas sensitivity

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【作者】 姜秀榕沈水发潘海波陈耐生

【Author】 JIANG Xiu-rong,SHEN Shui-fa,PAN Hai-bo,CHEN Nai-sheng(College of Chemistry and Chemical Engineering,Fuzhou University,Fuzhou,Fujian 350002,China)

【机构】 福州大学化学化工学院福州大学化学化工学院 福建福州350002福建福州350002

【摘要】 应用双微乳液法,在聚乙二醇辛基苯基醚(TX100)/正己醇/环己烷/水体系的W/O型微乳液中合成了掺锡和金的氧化铁前驱体,考察了主要制备条件对前驱体粒径的影响,对前驱体经400℃灼烧后所得的粉体进行了表征和气敏性测试,表明制得的共同掺杂5%mol Sn4+和0.5%mol Au3+的粉体对C2H5OH气体有较好的气敏性.

【Abstract】 The Sn/Fe2O3 and Sn/Au/Fe2O3 particles were prepared in W/O microemulsion system containing TX100/n-hexanol/cyclohexane/H2O.Some factors that affected size distribution of the precursor,such as the content of water phase,ratio of surfactant to cosurfactant and ratio of surfactant to oil phase were investigatied.The calcined particles were characterized with XRD.The measurement of gas sensitivity revealed that the material doped with 5%mol Sn+-0.5%mol Au+ exhibited good gas sensing response to C2H5OH at a low heating current.

【关键词】 微乳液法Fe2O3纳米粉体气敏性
【Key words】 microemulsionFe2O3nano powdergas sensitivity
【基金】 福建省教育厅科研资助项目(K02011);福州大学科技发展基金资助项目(XKJ(YM)-0101)
  • 【文献出处】 福州大学学报(自然科学版) ,Journal of Fuzhou University(Natural Science Edition) , 编辑部邮箱 ,2007年01期
  • 【分类号】O614.811
  • 【被引频次】7
  • 【下载频次】287
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