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瓯柑石油醚提取物的GC-MS分析

Analysis of extractives by petroleum from Cilrus suavissima Hort.et Tanaka by GC-MS

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【作者】 杨小凤仇佩虹李永林丽艾常春

【Author】 YANG Xiao-feng~,QIU Pei-hong,LI Yong,LIN Li and AI Chang-chun (Departmemt of Chemistry,Wenzhou Medical College,Wenzhou 325035)

【机构】 温州医学院药学院化学教研室温州医学院药学院化学教研室 温州325035温州325035

【摘要】 为了研究瓯柑的挥发性成分和脂溶性成分,采用GC-MS分析法进行分离鉴定,并用面积归一法确定各成分的质量分数。从瓯柑果肉石油醚提取物中分离鉴定出11种成分,占总提取物的97.43%,其主要成分为(Z,Z)-9,12-十八碳二烯酸(37.46%)、γ-谷甾醇(22.91%);从瓯柑皮石油醚提取物中分离鉴定出10种成分,占总提取物的99.79%,其主要成分为柠檬烯(86.39%)。

【Abstract】 To analyze the volatile and liposoluble constituents extracted from Cilrus suavissima Hort.et Tanaka,the components were separated and identified by GC-MS,and its contents were determined with area normalization method.11 compounds were separated and identified,97.43% by weight of the extractives from the pulp,and 10 compounds were determined from the extractives of the rind,99.79% by weight.Main compounds in the extractives from the pulp were 9,12-Octadecadienoic acid(Z,Z)(37.458%) and gamma.-Sitosterol(22.913%),limonene(86.39%) from the rind.

【基金】 温州市科技局科研基金(Y2004A020)项目资助
  • 【文献出处】 分析试验室 ,Chinese Journal of Analysis Laboratory , 编辑部邮箱 ,2007年01期
  • 【分类号】R284
  • 【被引频次】18
  • 【下载频次】296
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