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超大挤压变形对钛合金增强镁基复合材料显微组织的影响
Effect of Ultra-Deformation on the Microstructures of Titanium Alloy Reinforced Magnesium Matrix Composites
【摘要】 采用粉末冶金法制备了钛合金(Ti-6Al-4V)(质量分数,下同)颗粒增强MB15镁基复合材料,经225:1的超大比热挤变形后,借助光学显微镜(OM)、扫描电镜(SEM)和透射电镜(TEM)对其显微组织进行了研究。结果表明:钛合金颗粒沿挤压方向因塑性变形而被拉长,其增强效果得到提高;超大比热挤变形能够显著细化基体晶粒,并提高复合材料的组织均匀性;此外,原镁粉表面的氧化膜经超大比变形后得到了有效的碎化和分散,具有一定的弥散强化效果,因此可充当粉末冶金制备镁基复合材料的辅助增强相。
【Abstract】 Magnesium matrix composite reinforced by titanium alloy (Ti-6Al-4V) particulate was fabricated by powder metallurgy route. The samples of composite were hot-extruded with an ultra-deformation ratio of 225:1. The microstructures of extruded samples were investigated using optical microscopy, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The results showed that the Ti-6Al-4V particulates were apparently elongated along the extrusion direction, thus increased its reinforcing effect on the matrix. The ultra-deformation could markedly decrease the grain sizes of the composite matrix, and greatly improve the homogeneity of microstructures when compared with a lower ratio of extrusion deformation; in addition, the oxide layers on the surface of original Mg particles were effectively broken and dispersed randomly in the vicinity of Mg-Mg interfaces. It produced an oxidedispersion-strengthening (ODS) effect, further reinforced the matrix as a kind of secondary reinforcement.
【Key words】 titanium alloy; magnesium matrix composite; hot extrusion; microstructure;
- 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2007年05期
- 【分类号】TB331;TG113.12
- 【被引频次】2
- 【下载频次】276