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超声萃取-色谱分离农残检测样品前处理方法及装置研究
Pretreatment Method and Installation Research of Pesticide Residue Testing Samples
【摘要】 结合农业部NY/T761.1-2004标准,利用超声法和固相萃取联用法,将自制的前处理装置用于蔬菜农药残留检测中样品的快速前处理,配合后续的气相质谱联用仪(GC-MS),提高了农药残留的检测效率。此装置可连续一体化完成搅碎蔬菜、提取残留农药、净化等操作,具有快速、简便等特点,适用于较大规模批发市场中蔬菜农药残留的快速检测。
【Abstract】 Combined with agriculture department standard NY/T 761.1-2004,the self-made pretreatment device was applied in rapid preparation of pesticide residues in vegetable samples using ultrasonic and solid-phase extraction method.The device could cooperate with the following GC-MS and improve detection efficiency of pesticide residues.This device could whisk vegetables,extract pesticide residues and purify it,which was simple and convenient and could be used for vegetable rapid detection in large-scale wholesale market.
【关键词】 装置;
前处理;
超声波;
固相萃取;
农药残留;
【Key words】 Device; Pretreatment; Ultrasonic; Solid-phase extraction; Pesticide residue;
【Key words】 Device; Pretreatment; Ultrasonic; Solid-phase extraction; Pesticide residue;
【基金】 安徽省“十一五”科技攻关计划项目资助
- 【文献出处】 安徽农业科学 ,Journal of Anhui Agricultural Sciences , 编辑部邮箱 ,2007年17期
- 【分类号】S481.8
- 【被引频次】10
- 【下载频次】432