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动物中药材全蝎的粉末X射线衍射Fourier图谱鉴定

Identification of Traditional Chinese Medicine Scorpio by Powder X-ray Diffraction Fourier Pattern

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【作者】 翁立明吴云山吕扬王树春郑笑为张继朱志峰

【Author】 WENG Li-ming,WU Yun-shan,LvYang #,WANG Shu-chun *,ZHENG Xiao-wei *,ZHANG Ji *,ZHU Zhi-feng * *(Department of Analysis,Institute of Materia Medica,CAMS and PUMC,Beijing 100050,China)*Department of Pharmacy,Shaanxi Medical Higher School,Xi an 710068;**Department of Chinese Traditional Medicine,National Institute for the Control of Pharma ceutical and Biological Products,Beijing100050;***Departmentof Chinese Traditional Medicine,Shaanxi Provincial Institute for DrugControl,Xi an710061

【机构】 中国协和医科大学中国医学科学院药物研究所分析室中国协和医科大学中国医学科学院药物研究所分析室 北京100050北京100050

【摘要】 目的建立动物中药材全蝎的鉴定分析新方法。方法用X射线衍射Fourier图谱分析技术对湖北、陕西、山东等不同产地的10个全蝎样品进行分析研究,获取全蝎中药材的对照粉末X射线衍射Fourier指纹图谱。结果除7#样品外,其他9个样品衍射图谱的几何拓扑图形基本一致。9个全蝎样品(除7#)共有11个特征标记峰。结论X射线衍射Fourier指纹图谱鉴定法可用于动物中药材全蝎样品的分析鉴定和质量控制。

【Abstract】 Objective To set up a new analysis method of the traditional Chinese medicine Scorpio.Methods Ten Scorpio samples were obtained from Hubei,Shaanxi,and Shandong provinces and analyzed with X-ray diffraction Fourier pattern technique to obtain the geometric topology and characteristic marked peak of Scorpio.Results The geometric topologies of 9 samples were similar,excepting Sample 7 #.Totally 11 characteristic marked peaks were observed among these 9 samplies.Conclusion X-ray diffraction Fourier pattern is a useful tool for the identification and quality control of the Scorpio.

【基金】 科技部专项基金(科01-3)~~
  • 【文献出处】 中国医学科学院学报 ,Acta Academiae Medicinae Sinicae , 编辑部邮箱 ,2006年05期
  • 【分类号】R284.1
  • 【被引频次】15
  • 【下载频次】254
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