节点文献
中药马钱子中毒死亡检验方法的研究
Determination by GC-NPD and GC-MS of Traditional Chinese Medicine of Semen Strychnine
【摘要】 目的建立人体生物检材中的士的宁和马钱子碱的检测方法。方法用GC/NPD及GC/MS检测马钱子药渣,喝剩的马钱子药液及人体肝脏中士的宁和马钱子碱。结果建立了多种样品中士的宁和马钱子碱的定性、定量分析方法。结论本方法操作简便,定性定量准确,可靠。用此方法可以准确测定生物检材(肝脏等)的士的宁和马钱子碱含量。
【Abstract】 OBJECTIVE To establish the determination method of strychnine and vauqueline in biological materials such as drug residues, the remaining drug solution and human liver.METHOD The GC-NPD and GC-MS was used to determine the contents of strychnine and vauqueline.RESULT A reliable quantitative and qualitative determination method was established.CONCLUSION The method can be used to determine strychnine and vauqueline in biological materials (in liver et al).
【关键词】 士的宁;
马钱子碱;
气相色谱氮磷检测器;
气相色谱-质谱;
定性定量分析;
【Key words】 strychnine; vauqueline; GC-NPD; GC-MS; quantitative and qualitative determination method;
【Key words】 strychnine; vauqueline; GC-NPD; GC-MS; quantitative and qualitative determination method;
- 【文献出处】 中国药学杂志 ,Chinese Pharmaceutical Journal , 编辑部邮箱 ,2006年21期
- 【分类号】D919
- 【被引频次】4
- 【下载频次】212