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毛老虎叶子挥发油的GC-MS分析

Extraction of essential oil from Hyptis Suaveolens(L.) Piot.leaves and components analysis by GC-MS

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【作者】 黄秀香林翠梧韦滕幼韦万兴黄克建

【Author】 HUANG Xiu-xiang~(1,2),LIN Cui-wu~(1*),WEI Teng-you~1,WEI Wan-xing~1,HUANG Ke-jian~3(1.School of Chemistry and Chemical Engineering,Guangxi University,Nanning 530004,China;2.Department of Chemistry and Life Sciences Hechi(University),Yizhou 546300,China;3.The Public Security Department of Guangxi,Nanning 530000,China)

【机构】 广西大学化学化工学院广西公安厅 广西南宁530004河池学院化学与生命科学系广西宜州546300广西南宁530004广西南宁530012

【摘要】 目的:提取毛老虎叶子挥发油并分析研究其化学成分。方法:采用水蒸气蒸馏法提取,馏出液先用;醚萃取得到挥发油(Ⅰ),再用乙酸乙酯进一步提取得挥发油(Ⅱ),并通过GC/MS技术对其进行分析。结果:共分离鉴定出化学成分78个,其中挥发油(Ⅰ)鉴定出68种化合物,挥发油(Ⅱ)鉴定出25种化合物。结论:挥发油的主要成分为1.8-桉树脑、石竹烯、2,6,6-三甲基二环[3.1.1]庚-2,3-二醇等化合物。

【Abstract】 AIM: The essential oil was extracted from Hyptis suaveolents(L.) Piot leaves and the chemical components were analyzed. METHODS: The essential oil was extracted by steam distillation.Then the distillate was treated with ether and essential oil was obtained(Ⅰ).Then surplus oil distillate was extracted with ethyl acetate and essential oil was got(Ⅱ).Essential oil was analyzed by GC/MS. RESULTS: 78 compounds were identified in total.68 compounds were identified from essential oil(Ⅰ).25 compounds were detected from essential oil(Ⅱ). CONCLUSION: The principle constituents of the essential oil are 1.8-Cineole、 Caryophyllene、 Bicyclo(3.1.1) heptane-2,3-diol,2,6,6-trimethyl-etc.

【基金】 广西科技攻关项目(桂科攻0480005)
  • 【文献出处】 中成药 ,Chinese Traditional Patent Medicine , 编辑部邮箱 ,2006年08期
  • 【分类号】R284
  • 【被引频次】6
  • 【下载频次】173
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