节点文献
几个新型含氟化合物的合成
Synthesis of Several Novel Fluorinated Compounds
【摘要】 以3-硝基-4-氯三氟甲苯(1)为起始原料,合成了新型含氟杂环化合物8和3个含氟中间体4,5,6.通过IR,NMR,MS和元素分析对它们的结构进行了表征.探讨了反应条件对产物结构的影响,提出了化合物4可能的形成机理.
【Abstract】 The synthesis of fluorinated heterocycle 8 and the three intermediates 4,5 and 6 was first re-ported.The structures were determined by IR,NMR,MS spectra and elemental analysis.The influence of reaction conditions was explored and the possible mechanism of the formative of 4 was discussed.
【关键词】 3-硝基-4-氯三氟甲苯;
含氟化合物;
杂环;
合成;
【Key words】 3-nitro-4-chlorobenzotrifluoride; fluorinated compound; heterocycle; synthesis;
【Key words】 3-nitro-4-chlorobenzotrifluoride; fluorinated compound; heterocycle; synthesis;
【基金】 湖南省教育厅重点(No.02A036);湖南省科技计划(No.03JZY3042)资助项目.
- 【文献出处】 有机化学 ,Chinese Journal of Organic Chemistry , 编辑部邮箱 ,2006年06期
- 【分类号】O621.25
- 【被引频次】2
- 【下载频次】417