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SiC/C功能梯度材料的设计、制备及性能

Design,Fabrication and Properties of SiC/C Functionally Graded Materials

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【作者】 张国兵郭全贵刘朗史景利宋进仁

【Author】 Zhang Guobing~(1,2) Guo Quangui~1 Liu Lang~1 Shi Jingli~1 Song Jinren~1(1 Key Laboratory of Carbon Materials,Institute of Coal Chemistry,Chinese Academy of Sciences,Taiyuan 030001)(2 Graduate School,Chinese Academy of Sciences,Beijing 100039)

【机构】 中国科学院山西煤炭化学研究所炭材料重点实验室中国科学院山西煤炭化学研究所炭材料重点实验室 太原030001中国科学院研究生院北京100039太原030001

【摘要】 采用粉末冶金法中的叠层法在2 000℃、40 MPa的热压烧结条件下制备了几类不同层数及成分分布指数的SiC/C功能梯度块体材料(FGM)。所得样品的结构扫描图表明材料总体梯度特征显著,相比四层FGM样品,八层(SF8)FGM样品梯度过渡趋于连续,其不同层间层界面相对模糊化,界面处的结合性能良好,与最初设计相吻合;500℃~室温循环淬水实验表明,采用参数优化设计的SF8(P=0.6)FGM有效地缓和了内部热应力,具有良好的抗热震性能。

【Abstract】 SiC/C block Functionally graded materials(FGMs) with different layers and compositional distribution factor(P) are designed and fabricated successfully by power stacking and hot-press sintering under a pressure of 40 MPa at 2 000℃.SEM micrographs show that all SiC/C FGMs as received have excellent gradient characteristics compared with that of four-layered FGM.Gradient characteristics of eight-layered FGM have a continuous trend and its interfaces between different layers are crack-free and tightly combined.Thermal shock resistance of SiC/C FGM is repeatedly tested by water quenching with the temperature difference of 500℃.It seems that eight-layered SiC/C FGM(P=0.6) with optimized parameter has better thermal shock resistance and no cracks occur after 90 times quenching.

  • 【文献出处】 宇航材料工艺 ,Aerospace Materials & Technology , 编辑部邮箱 ,2006年S1期
  • 【分类号】TN304
  • 【被引频次】11
  • 【下载频次】401
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