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单扫描示波极谱法测定刺芒柄花素
Determination of Formononetin by Single Sweep Scillopolarography
【摘要】 报道了测定刺芒柄花素的单扫描示波极谱方法,在0.02mol/L的HAc ̄NaAc缓冲溶液(pH=5.35)中,刺芒柄花素在-1.34v(vs.SCE)处有一灵敏的二阶导数还原峰,峰电流与刺芒柄花素浓度在4.0×10-7~4.8×10-6mol/L范围内具有良好的线性关系(r=0.9955,n=6),检出限为2.0×10-7mol/L。用该方法测定刺芒柄花素,结果令人满意。
【Abstract】 A method for the polarogrphic determination of Formononetin is described,in NaAc-HAc of 0.02 mol/L buffer solution(pH= 5.35),two well-defined quadratic derivative waves at-1.34 v(vs.SCE),the peak current is linearly proportional to its concentration in the range from 4.0×0-7~4.8×0-6 mol/L(r=0.9955,n=6),the detection limit is 2.0×0-7 mol/L,the method was used to deterimine the content of Formononetin with satisfactory results.
【关键词】 单扫描示波极谱法;
刺芒柄花素;
峰电流;
【Key words】 single sweep oscillopolarography; formononetin; peak current;
【Key words】 single sweep oscillopolarography; formononetin; peak current;
【基金】 陕西省教育厅科研计划项目(04JK303)
- 【文献出处】 咸阳师范学院学报 ,Journal of Xianyang Normal University , 编辑部邮箱 ,2006年02期
- 【分类号】R284
- 【被引频次】1
- 【下载频次】92