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微波消解氢化物-原子荧光法同时测定土壤中的砷和汞
Synchronous mensuration os soil arsenic and hydrargyrum by using hydride generation-atomic fluorescence spectrometry digested with microwave
【摘要】 建立了氢化物-原子荧光法同时测定土壤中砷和汞的方法。在建立的最佳工作条件下,用微波消解处理样品,砷的回收率为90%~110%,汞的回收率为95%~105%,方法的检出限、精密度和准确度均能满足土壤检验的要求,可广泛地应用于各种环境土壤的检测。
【Abstract】 Method of mensurating soil Arsenic and Hydrargyrum simultaneously using microwave digestion hydride-atomic fluorescence spectrometry was setup.Under optimum conditions,the recovery rates of Arsenic and Hydrargyrum could be up to 90 %-100 % and 95 %-105 % respectively when samples was digested by microwave.The precision and accuracy accord with the requirement of soil test,which could be widely used in kinds of soil detection.
【关键词】 砷;
汞;
土壤;
微波消解;
原子荧光法;
【Key words】 arsenic; hydrargyrum; soil; microwave digestion; atomic fluorescence;
【Key words】 arsenic; hydrargyrum; soil; microwave digestion; atomic fluorescence;
- 【文献出处】 西南农业学报 ,Southwest China Journal of Agricultural Sciences , 编辑部邮箱 ,2006年02期
- 【分类号】X53
- 【被引频次】32
- 【下载频次】308