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河北卢龙地区青蒿挥发性化学成分的气相色谱-质谱分析

Study on Volatile Constituents of the Artemisia apiacea Hance From Lulong Area in Hebei Province by Gas Chromatography-Mass Spectrometry

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【作者】 赵丽娟辛广张捷莉

【Author】 ZHAO Li-juan,XIN Guang,ZHANG Jie-li(Department of Chemistry,Anshan Normal University,Anshan 114005,China)

【机构】 鞍山师范学院鞍山师范学院 辽宁鞍山114005辽宁鞍山114005

【摘要】 采用普通水蒸气蒸馏萃取法,对产自河北卢龙地区青蒿中的挥发油进行提取,测得青蒿挥发油含量为7.2%;并用气相色谱-质谱(GC/MS)联用技术进行分析鉴定,结合计算机质谱图库检索技术对分离的化合物进行结构分析,鉴定21种化学组分,占总挥发性物质总含量的74.02%。应用峰面积归一化法确定了各成分的相对含量。结果表明:普通水蒸气蒸馏萃取法提取的挥发油中主要含有N,N?-双(2,6-二甲基-6-亚硝基)庚-2-烯-4-酮(29.29%)、桉叶油素(7.16%)、二十六烷(5.93%)、二十五(碳)烷(5.1%)等。

【Abstract】 The volatile oil was extracted from the Artemisia apiacea Hance from Lulong area in Hebei Province by using direct distillation extraction method(DDE).The content of the volatile oil was 7.2%.21 compounds were identified by GC/MS.The contents of the identified compounds made up to 74.02% of total volatile substances.The relative content of the components were determined with area normalization method.The main components of volatile substances are N,N′-Bis(2,6-dimethyl-6-nitrosohept-2-en-4-one)(29.29%)、Eucalyptol(7.16%)、Hexacosane(5.93%)、Pentacosane(5.1%),etc.

  • 【文献出处】 时珍国医国药 ,LiShiZhen Medicine and Materia Medica Research , 编辑部邮箱 ,2006年09期
  • 【分类号】R284
  • 【被引频次】6
  • 【下载频次】155
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