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长春七中总香豆素提取工艺研究
Technology Research on Extracting Total Cumarin From Radix Sesali
【摘要】 目的筛选长春七总香豆素的最佳提取工艺。方法采用正交实验设计L9(34)考察乙醇浓度、乙醇用量、提取时间、提取次数4个因素对提取工艺的影响,以蛇床子素为对照品,用UV-1102型紫外-可见分光光度计测定总香豆素含量。结果长春七中总香豆素含量的最佳提取工艺为D3A3B2C1即:55%乙醇,5倍药材量乙醇体积,提取3次,每次1 h。结论本方法工艺合理,可为工业化大生产提供参考。
【Abstract】 Objective To select the maximal technology of extracting total cumarin from Radix Sesali.Method According to orthogonal test design L9(34),observed effect on the technology of the four following factors-ethanol concentration,ethanol content,extracting time and number of extracting times.Then with substance of Fructus Cniidii as control product,determined content of total cumarin using UV-1102 ultraviolet-visible spectrophotometer.Result The best technology is D3A3B2C1,that is,55% ethanol,ethanol volume of five times the raw drugs,three times of extracting,and 1 hour a time.Conclusion the technology is rational as to be referential for industrialized production.
- 【文献出处】 陕西中医学院学报 ,Journal of Shaanxi College of Traditional Chinese Medicine , 编辑部邮箱 ,2006年04期
- 【分类号】R284.2
- 【被引频次】9
- 【下载频次】505