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机械球磨与热处理法制备FeAl(B2)金属间化合物粉末
Preparation of FeAl(B2) intermetallic powder by ball milling and heat treatment
【摘要】 F eA l金属间化合物在高温结构材料领域有广阔的应用前景。该文采用机械球磨与热处理工艺制备适于注射成形的F eA l金属间化合物粉末,利用X射线衍射仪和扫描电子显微镜研究了球磨和热处理过程中F e-A l(xA l=48%)粉末的物相结构和粉末形貌的变化规律。结果表明,F e-A l混合粉末经12 h球磨,可制得粒径为30μm左右的近球形F e(A l)和A l(F e)固溶体粉末;经进一步真空热处理后,粉末物相转变为以F eA l(B2)为主的金属间化合物。
【Abstract】 FeAl intermetallics are excellent candidates for high temperature structural materials.A FeAl(B2) intermetallic powder that can be used for injection molding was prepared by ball milling and heat treatment.The microstructural and morphological characteristics of the Fe-Al(xAl=48%) powder were analyzed by X-ray diffraction and a scanning electron microscope.The results show that,after being milled for 12 h,the Fe-Al powder is spherical with a mean particle size of 30 μm.After vacuum annealing,the FeAl(B2) intermetallic phase forms and dominates in the powder microstructure.
【Key words】 heat treatment; FeAl; intermetallic; ball milling; powder;
- 【文献出处】 清华大学学报(自然科学版) ,Journal of Tsinghua University(Science and Technology) , 编辑部邮箱 ,2006年08期
- 【分类号】TB44
- 【被引频次】13
- 【下载频次】318