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3%甲胺基阿维菌素B1a苯甲酸盐微乳剂高效液相色谱分析
Analysis of emamectin benzoate 30 ME by HPLC
【摘要】 采用ZrobaxXDBC18色谱柱,以乙腈-水(体积比为70∶30),加入0.5%三乙胺,用乙酸调节pH值8.5为流动相,在245nm紫外波长下对3%甲胺基阿维菌素B1a苯甲酸盐微乳剂进行高效液相色谱法分析,以外标法测定。变异系数为0.56%,回收率为99.7%,线性相关系数为0.9999。
【Abstract】 Quanlitative analysis of emamectin benzoate 30 ME was established by HPLC with Zrobax XDB C18 atUV 245nm using acetonitrile, water and triethylamine as mobile phase(pH 8.5), external standard method. The resultsshowed that the coefficient of variation and ratio of recovery were 0.56% and 99.7% respectively, the liner correlationcoefficient was 0.9999.
【基金】 国家“粮食丰产科技工程”项目(2004BA520A15-4)
- 【文献出处】 农药 ,Agrochemicals , 编辑部邮箱 ,2006年12期
- 【分类号】TQ453.2
- 【被引频次】1
- 【下载频次】109