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不同方法对提取原煤中PAHs分布的影响

Impact of different extracting method on distribution of PAHs in raw coal

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【作者】 薛翦刘桂建张浩原钮志远郑刘根

【Author】 XUE Jian,LIU Gui-jian,ZHANG Hao-yuan,NIU Zhi-yuan,ZHENG Liu-gen(School of Earth and Space Science,University of Science and Technology of China,Hefei 230026,China)

【机构】 中国科学技术大学地球与空间科学学院中国科学技术大学地球与空间科学学院 安徽合肥230026安徽合肥230026

【摘要】 选取超声提取法和索氏提取法,对淮北煤田主采煤层新鲜煤样中多环芳烃进行提取,并利用气相色谱-质谱联用仪对提取液中的多环芳烃进行定量分析,研究了不同方法对提取原煤中(US-EPA)优先控制的多环芳烃种类、质量分数和分布的影响。结果表明,在本实验条件下索氏提取法在提取原煤中多环芳烃能力上优于超声提取法。

【Abstract】 The samples collected from the fresh raw coals in Huaibei coalfield were extracted by Soxhlet extracting method and ultrasonic-assisted extraction method respectively.The extracted liquids were determined by GC-MS.And the concentrations of PAHs attented by USEPA were analyzed.The impact on the concentration and distribution of PAHs extracted by different extracting methods from raw coal were studied.The study results indicated that the ability of Soxhlet extraction method to extract PAHs from raw coal is better than that of ultrasonic extraction method under the experimental condition suggested in this paper.

【基金】 国家自然科学重点基金(40273035);安徽省优秀青年基金(04045064);中国科技大学研究生创新基金(KD2005032)资助
  • 【文献出处】 煤田地质与勘探 ,Coal Geology & Exploration , 编辑部邮箱 ,2006年04期
  • 【分类号】TQ533
  • 【被引频次】9
  • 【下载频次】213
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