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对甲基苯磺酰异氰酸酯的稳定性考察

STUDY ON THE STABILITY OF p-METHYL BENZENESULFONYL ISOCYANATE

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【作者】 王向军姚彤炜曾苏

【Author】 WANG Xiang-jun,YAO Tong-wei,ZENG Su(Research Lab.of Pharmacology Analysis,College of Pharmacology,Zhejiang University,Hangzhou 310031,China)

【机构】 浙江大学药学院药物分析研究室浙江大学药学院药物分析研究室 杭州310031杭州310031

【摘要】 采用气相色谱法测定对甲基苯磺酰异氰酸酯,按峰面积归一化法计算含量,稳定性试验表明,对甲基苯磺酰异氰酸酯在高温、氧气环境下稳定,而在光、潮湿环境下极不稳定,样品应在干燥、密闭、避光和充氮气条件下贮存。

【Abstract】 Gas chromatographic method was used for the determination of p-methyl benzenesulfonyl isocyanate(MBSIC),the content was calculated by the method of normalized peak area.Experimental results showed that MBSIC was stable in atmosphere of oxygen and under high temperature,but unstable to light irradiation and moisture.Sample of MBSIC should be stored in dry and closed container filled with nitrogen and placed in dark place.

  • 【文献出处】 理化检验(化学分册) ,Physical Testing and Chemical Analysis(Part B:Chemical Analysis) , 编辑部邮箱 ,2006年06期
  • 【分类号】O657.71;O625.7
  • 【下载频次】211
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