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椿乳凝胶质量控制方法研究

Quality control standard for Chunru gel

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【Author】 ZHANG Jie~1,GONG Yun~2,XIANG Da-xiong~(3#),LUO Jie-ying~4,ZHOU Chunshan~5(1 The Third Xiangya Hospital,Central South University,Hunan 410013)(2 Zhuzhou Qianjin Pharmaceutical Co.Ltd.,Hunan 412003)(3 The Second Xiangya Hospital,Central South University,Hunan 410011)(4 School of Chinese Meteria Medical,Hunan College of Chinese Medicine 410007)(5 Chemical and Chemical Industry College,Zhongnan University,Hunan 410083)

【机构】中南大学湘雅三医院；株洲千金药业股份有限公司；中南大学湘雅二医院临床药学研究室；湖南中医学院药学院；中南大学化学化工学院湖南410013；湖南412003；湖南410011；湖南410007；湖南410083；

【摘要】目的制定椿乳凝胶质量标准。方法采用薄层色谱法(TLC)鉴别牡丹皮和冰片,高效液相色谱法(HPLC)测定苦参碱的含量。结果薄层斑点清晰,重现性好;椿乳凝胶中苦参碱平均加样回收率为97.94%,RSD为3.16%。结论本法简便、准确,可有效控制椿乳凝胶质量。更多还原

【Abstract】 Objective To set down the quality control standard for Chunru gel.Methods Cortex Moutan and Borneolum syntheticum were identified by thin layer chromatography(TLC),and the content of matrine was determined by HPLC.Result The result showed that the spots of TLC were fairly clear,the repeatability was good and the average sample-adding recovery of matrine was 97.94%(RSD=3.16%).Conclusion The method is simple,accurate and qualified for the quality control of Chunru gel effectively.更多还原

【关键词】椿乳凝胶；苦参碱；高效液相色谱；丹皮酚；冰片；薄层色谱；
【Key words】 Chunru gel； matrine； HPLC； paeonolum； borneolum syntheticum； thin layer chromatography；

【基金】湖南省科技厅重大科技专项(No.04SK1010)

【文献出处】北京中医药大学学报 ,Journal of Beijing University of Traditional Chinese Medicine , 编辑部邮箱 ,2006年02期

【分类号】R286
【被引频次】2
【下载频次】187

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