【摘要】 以对甲基氯化苄与二甲基烯丙基胺为原料合成了二甲基烯丙基对甲基苄基氯化铵,考查了光照、氮气保护、避光、温度、原料配比、反应时间和不同溶剂等因素对反应的影响,通过四苯硼钠的定量分析确立了最佳反应条件,并对产物的结构进行了表征.更多还原

【Abstract】 Dimethyl allyl pmethylbenzyl ammonium chloride was synthesized from pmethylbenzyl chloride and dimethyl allylamine.The factors affecting the reaction,such as temperature,reaction composition,reaction time,solvent and so on were investigated.The yields were determined by gravimetric analysis with NaBPh₄.The structure of the product was characterited by IR,¹H NMR and MS.更多还原