【摘要】 通过苯酚和碳酸二甲酯的酯交换反应合成了碳酸甲苯酯,采用减压精馏对其进行了分离提纯,得到纯度>99.5%的碳酸甲苯酯;运用红外光谱、紫外光谱、核磁共振氢谱以及质谱对其结构进行了表征,并对其光谱数据进行了解析。更多还原

【Abstract】 Methyl phenyl carbonate(MPC) was prepared by transesterification of dimethyl carbonate(DMC) with phenol and the product with a purity exceeding 99.5% was obtained by vacuum distillation.The structure of the product was identified to be MPC by IR,UV,(()~1HNMR),MS spectrometry,and the spectral data were interpreted.更多还原