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烤烟叶片发育过程中阴离子的离子色谱法测定研究

The Determination of Flue-cured Tobacco Leaves Anions During Its Growth Development by Ion Chromatography

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【作者】 杜惠文韦凤杰杨卫芳黄晓书刘国顺

【Author】 DU Hui-wen1,WEI Feng-jie2,YANG Wei-fang1,HUANG Xiao-shu3,LIU Guo-shun2(1.Anyang Environmental Monitoring Centre Office of Henan Province,Anyang 455000,China;2.College of Agronomy Henan Agricultural University National Tobacco Cultivation?Physiology and Biochemistry Research Center,Zhengzhou 450002,China;3.Key Discipline and Open Laboratory of Agricultural Biological and Engineering Technique of Henan Higher Learning Institute,Zhengzhou 450002,China)

【机构】 河南省安阳市环境监测中心站河南农业大学国家烟草栽培生理生化研究基地河南省高等学校农业生物技术与工程技术重点学科开放实验室河南农业大学国家烟草栽培生理生化研究基地 河南安阳455000郑州450002河南安阳455000

【摘要】 研究了离子色谱法测定烤烟叶片中阴离子的方法.色谱条件:淋洗液为0.003mol/LNa2CO3和0.006mol/LNaHCO3混合液,淋洗液流速1.0ml/min.结果表明方法可同时精确测定6种阴离子,相对标准偏差RSD0.58%-2.41%,样品加标回收率在93%-110%之间.用该方法研究了烤烟叶片中的阴离子含量,结果令人满意.

【Abstract】 A ion chromatography method for the determination of flue-cured tobacco leaf anions was studied.The separation of the anions was achieved in an 0.003 mol/L Na2CO3~0.006 mol/LNaHCO3 and a flow rate 1.0ml/min as gradient eluant.The method is simple and useful and has good linearity with correlation coefficients and determination 6 kinds anions at the same time.The recoveries of flue-cured tobacco leaves anions are 93%-110%,and relative standard deviations are 0.58%-2.41%.This method was applied to determine anions in flue-cured tobacco leaves during the course of developing phase with satisfactory result.

【基金】 国家烟草专卖局项目(110200201005)
  • 【分类号】S572
  • 【下载频次】51
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