节点文献
化学共沉淀法制备纳米In2O3粉末
Nano-sized In2O3 Powder Prepared by Chemical Precipitation Method
【摘要】 纳米In2O3粉末是一种用途广泛的多功能材料。以金属铟为原料,采用化学共沉淀法制得了氢氧化铟沉淀物。经过干燥,并且在不同温度下煅烧,可以制得纳米In2O3粉末。运用差热分析(DTA)、X射线衍射(XRD)、透射电镜(TEM)、电阻测试等观测手段对粉末进行了表征。比较系统地研究了热处理温度对粉末性能的影响,得出最适宜的热处理温度为700°C。
【Abstract】 Nano-sized In2O3 powder is a widely used multifunctional material.Metal indium was first dissolved in HCl;the solution was then neutralized by ammonia;In(OH)3 precipitate was the final product of neutralization and precipitation.After drying and roasting at different temperatures nano-sized In2O3 powder was obtained.The powder was characterized by differential thermogravimetric analysis(DTA),X-ray diffraction(XRD),transmission electron microscopy(TEM) and resistant testing.The most feasible temperature was 700(°C).
【关键词】 纳米In2O3粉末;
化学共沉淀法;
粉末制备;
粉末性能;
热处理温度;
【Key words】 nano-sized In2O3 powder; chemical precipitation method; powder preparation; powder properties; heating temperature;
【Key words】 nano-sized In2O3 powder; chemical precipitation method; powder preparation; powder properties; heating temperature;
- 【文献出处】 华东理工大学学报(自然科学版) ,Journal of East China University of Science and Technology(Natural Science Edition) , 编辑部邮箱 ,2006年01期
- 【分类号】O614.372
- 【被引频次】9
- 【下载频次】221