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树脂法纯化茶多酚工艺的研究

Study on Purification of Tea Polyphenols with Macroporous Resins

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【作者】 高彦华刘晓娜乔喜芹

【Author】 Gao Yanhua Liu Xiaona Engineering Research Center of Plant Medical, Northeast Forestry University, (Harbin 150040) Qiao Xiqin Department of Pharmaceutical Engineering, Harbin University of Commerce, (Harbin 150076)

【机构】 东北林业大学植物药工程研究中心哈尔滨商业大学制药工程系 哈尔滨150040哈尔滨150040

【摘要】 目的:筛选适合制备高纯度茶多酚的树脂及其条件,以期得到纯度为98%茶多酚产品。方法:以茶多酚含量为指标.考察不同树脂对茶多酚吸附解吸特性,筛选出适合制备高纯度茶多酚的最佳工艺条件。结果:纯度为 35%,浓度为5mg/ml的茶多酚经H1020树脂吸附,吸附率达80.33%,依次经蒸馏水和10%的乙醇溶液洗脱除杂后, 80%乙醇洗脱,洗脱率达83.5%,洗脱液过滤后,经喷雾干燥得到纯度为98%以上的茶多酚产品。结论:为高纯度茶多酚的生产提供一种操作简单、产品质量高、生产成本低的绿色工艺。

【Abstract】 Objective: To select optimum process parameters of the purification of tea polyphenols with different macroporous adsorption resins to gain tea polyphenol with purity 98%. Methods: H1020 type macoroporos resign is considered as optimum resign for purification of Tea polyphenols.Results:The initial sample with the tea polyphenol purity35% was prepared to be 5mS/ml solution, then adsorbed by the optimal resin H1020, and eluted with double distilled water, 10%ethanol firstly and then eluted with 80%ethanol.The desorption ratio was 83.5% .The elution was boiled and granulated by spraying torrefaction.Then we got the product of tea polyphenol with purity 98% .Conclusion:This study provided a simple, high purification and low cost green process.

【关键词】 茶多酚树脂纯化
【Key words】 tea polyphenolsmacroporous resinpurification
  • 【文献出处】 黑龙江医药 ,Heilongjiang Medicine Journal , 编辑部邮箱 ,2006年02期
  • 【分类号】TQ461
  • 【被引频次】15
  • 【下载频次】433
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