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X射线荧光光谱法测定土壤及底泥中多种元素

To Measure Variety Elements in the Soil and Mud by X-ray Fluorescence Spectrographic

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【作者】 陈素兰胡冠九周春宏陈波章勇范迪富廖启林

【Author】 CHEN Su-lan~1,HU Guan-jiu~1,ZHOU Chun-hong~1,CHEN Po~1,ZHANG Yong~1,FAN Di-fu~2,LIAO Qi-lin~2(1.Jiangsu Environmental Monitoring Center,Nanjing,Jiangsu 210036,China;2.Jiangsu Province Geological Survey Institute,Nanjing,Jiangsu 210018,China)

【机构】 江苏省环境监测中心江苏省地质调查研究院江苏省地质调查研究院 江苏南京210036江苏南京210036江苏南京210018

【摘要】 采用粉末压片、X射线荧光光谱法测定土壤及底泥样品中铜、铅、铬、锌、镍等多种元素。优化了测量条件,采用理论α系数法校正基体效应,校准样品校正谱线重叠干扰,经标准样品及不同分析方法验证,该方法定量准确,分析速度快,精密度和准确度均符合要求。

【Abstract】 This article determined variety elements in soil and mud sample,such as Copper,Lead,Chromium,Zinc,Nickel with the powder sheeting and X-ray fluorescence spectrographic methods determination.The survey condition was optimized and the theory alpha method of correlates adjustment substrate effect was applied,the calibration sample overlapped with adjustment spectral line.The result showed this method was quota accurate and quick,and the accuracy was requirement for practice with confirmation by standard sample and different analysis method.

【关键词】 元素土壤底泥X射线荧光光谱法
【Key words】 ElementsSoilMudX-ray fluorescence spectrographic
【基金】 江苏省国土生态地球化学调查基金资助项目(20031230008和200312300009-03)
  • 【文献出处】 环境监测管理与技术 ,The Administration and Technique of Environmental Monitoring , 编辑部邮箱 ,2006年04期
  • 【分类号】X833;O657.34
  • 【被引频次】20
  • 【下载频次】230
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