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乙二胺-水体系中合成氧化锌纳米带
Synthesis of Zinc Oxide Nanobelts in Aqueous Solution of Ethylene Diamine
【摘要】 以乙二胺为介质,采用溶剂热法,在乙二胺-水体系中合成出宽度为20~30nm、长度为500~600nm的氧化锌纳米带,并进行了表征.在反应过程中,氧化锌纳米带通过“溶解-结晶”机制形成,溶剂乙二胺的配位是氧化锌纳米带形成的关键因素,通过调整NaOH用量控制溶液碱度,实现了氧化锌纳米带的取向生长.
【Abstract】 Zinc oxide nanobelts were synthesized in aqueous solution of ethylene diamine by solvothermal synthesis and characterized at the same time.The width and length of zinc oxide nanobelts are 20~30 nm and 500~600 nm respectively.Zinc oxide nanobelts were prepared through dissolution-crystallization mechanism.Ethylene diamine bonding was a key factor in synthesis of zinc oxide nanobelts,and the oriented growth of zinc oxide was controlled by the quantity of sodium hydroxide.
【关键词】 氧化锌;
纳米带;
乙二胺;
溶剂热合成;
【Key words】 zinc oxide; nanobelts; ethylene diamine; solvothermal synthesis;
【Key words】 zinc oxide; nanobelts; ethylene diamine; solvothermal synthesis;
【基金】 国家高技术研究发展计划(863)基金资助项目(编号:2004AA001520)
- 【文献出处】 过程工程学报 ,The Chinese Journal of Process Engineering , 编辑部邮箱 ,2006年05期
- 【分类号】TB383.1
- 【被引频次】10
- 【下载频次】355