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微波辐照法制备高分子稳定的水溶性铂氧化物纳米颗粒
Preparation of Polymer-stabilized Water Soluble Nanoparticles of Platinum Oxide by Microwave Irradiation
【摘要】 采用微波辐照法制备了水溶性聚乙烯吡咯烷酮稳定的氧化铂纳米颗粒,并对产物进行了UV-Vis、TEM和XPS等表征。在调节反应溶液的pH值时,加入一定量的乙酸钠,所制得的纳米颗粒粒径小、分布窄、稳定性好。
【Abstract】 Polyvinylpyrrolidone(PVP)-stabilized PtO2 nanoparticles were prepared by using microwave irradiation in water solution,and were characterized by UV-Vis,TEM and XPS examinations.When sodium acetate was added for adjusting pH value of the solution,the nanoparticles had smaller particle size with narrower distribution and better stability.
【关键词】 微波法;
聚乙烯吡咯烷酮;
氧化铂;
纳米颗粒;
【Key words】 microwave; polyvinylpyrrolidone; platinum oxide; nanoparticle;
【Key words】 microwave; polyvinylpyrrolidone; platinum oxide; nanoparticle;
【基金】 国家民委科研基金项目(MZZ04005)
- 【文献出处】 化学与生物工程 ,Chemistry & Bioengineering , 编辑部邮箱 ,2006年12期
- 【分类号】TB383.1
- 【被引频次】7
- 【下载频次】135