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表面有丝状吸附物的氮化硼纳米管的制备(英文)

PREPARATION OF BORON NITRIDE NANOTUBES COATED WITH TINY HAIR-LIKE STRUCTURES

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【作者】 籍凤秋曹传宝许亚杰李杰

【Author】 JI Fengqiu 1,2, CAO Chuanbao1, XU Yajie 1, LI Jie1 ( 1.Research Center of Materials Science, Beijing Institute of Technology, Beijing 100081; 2.Department of Traffic Engineering, Shijiazhuang Railway Institute of Technology, Shijiazhuang 050043, China)

【机构】 北京理工大学材料科学研究中心北京理工大学材料科学研究中心 北京100081石家庄铁道学院交通工程分院石家庄050043北京100081

【摘要】 采用简单工艺,即:将块体氧化硼(B2O3)在氮气气氛中球磨后,在1200℃、流动的氨气中热处理,成功合成了表面有大量丝状吸附物的BN纳米管。纳米管为六方BN晶体且呈竹节形貌,其直径为80~120nm,长度近1μm。纳米管表面丝状的吸附层也是六方BN晶体,细丝的长度为100nm左右,直径不到10nm。

【Abstract】 Boron nitride nanotubes with tiny hair-like coatings were prepared by a simple process. The method involved milling boron oxide in nitrogen gas and heating the samples at 1 200 ℃ in the presence of flowing ammonia gas. The BN nanotube is a hexagonal crystal structure with a bamboo-like morphology. The diameters of as-synthesized nanotubes range from 80 nm to 120 nm and the lengths are up to 1 μm. The tiny hair-like coatings on the nanotubes are also hexagonal BN with typical lengths of about 100 nm and diameters less than 10 nm.

  • 【文献出处】 硅酸盐学报 ,Journal of the Chinese Ceramic Society , 编辑部邮箱 ,2006年01期
  • 【分类号】TB383.1
  • 【被引频次】1
  • 【下载频次】214
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