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满山香子挥发油的提取及其中水杨酸甲酯含量的测定
Extraction volatile oil from seeds of schisandra propinqua and gas chromatographic analysis of methyl salicylate in the volatile oil
【摘要】 满山香子经水蒸气蒸馏,用石油醚进行萃取,得到满山香子挥发油,得率为5.50%。采用气相色谱(GC)法测定满山香子挥发油中水杨酸甲酯含量。结果表明,该挥发油中水杨酸甲酯含量在4.2~50.0m g/mL范围内具有良好的线性关系,r=0.9996,平均回收率为98.23%,相对标准偏差为4.12%。
【Abstract】 Volatile oil of schisandra propinqua was extracted by water distillation and partitioned by petroleum ether.The content of methyl salicylate in the volatile oil of schisandra propinqua was determined by gas chromatography(GC).The result showed that the calibration curves were linear between 4.2~50.0mg/mL(r = 0.9996),the average recovery was 98.23%,RSD was 4.12%.
【关键词】 满山香;
挥发油;
水杨酸甲酯;
气相色谱;
【Key words】 Schisandra propinqua; Volatile oil; Methyl salicylate; Gas chromatography;
【Key words】 Schisandra propinqua; Volatile oil; Methyl salicylate; Gas chromatography;
【基金】 广西省自然基金项目(桂科自0339032)
- 【文献出处】 广西轻工业 ,Guangxi Journal of Light Industry , 编辑部邮箱 ,2006年03期
- 【分类号】R284
- 【被引频次】1
- 【下载频次】201