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乳糖-间苯二酚树脂胶粘剂的合成
Synthesis of lactose-resorcinol resin adhesive
【摘要】 以乳糖和间苯二酚为原料成功合成了绿色环保型酚醛树脂粘合剂;并用正交实验法获得了该树脂合成的最佳反应条件及固化条件:浓盐酸3mL(相当于总质量的2.1%),n(乳糖):n(间苯二酚)=4.5,催化剂无水硫酸铜质量2.1g(相当于总质量的1.3%),硝酸铵质量13g(相当于总质量的7.8%),反应时间4h,固化温度100℃左右。
【Abstract】 In this paper,the green thermosetting resorcinol-lactose resin was prepared successfully.The optimum conditions of the synthesis and curing reaction of resorcinol-lactose resin were obtained by orthogonal experimental method:HC1 3mL(2.1%),the mole ratio of lactose and resorcinol was 4.5,CUSO4 2.1g(1.3%), NH4NO3 13g(7.8%),reaction time was 4h,and curing temperature was about 100℃
【基金】 陕西省自然科学基金(2003B19)资助项目。
- 【文献出处】 中国胶粘剂 ,China Adhesives , 编辑部邮箱 ,2006年10期
- 【分类号】TQ433.43
- 【被引频次】15
- 【下载频次】226