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纳米氧化铈的制备及其抛光性能的研究

Preparation of nano-sized CeO2 and its polishing performances

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【作者】 张鹏珍雷红张剑平施利毅

【Author】 ZHANG Peng-zhen~1,2,LEI Hong~1,ZHANG Jian-ping~2,SHI Li-yi~1,2(1.Research Center of Nano-science and Nano-technology,Shanghai University,Shanghai 200444,China)(2.School of Sciences,Shanghai University,Shanghai 200444,China)

【机构】 上海大学纳米中心上海大学理学院上海大学纳米中心 上海200444上海200444

【摘要】 采用溶胶-凝胶法制备了纳米CeO2粉体,并采用XRD、TOF-SIMS对其进行了表征。结果表明平均晶粒度在13.3nm,粒度分布均匀。进而研究了纳米CeO2在玻璃基片抛光中的抛光性能。ZYGO形貌仪表明,抛光后其表面平均粗糙度值(Ra)可降低到0.6nm左右。原子力显微镜(AFM)在5μm×5μm范围内测得基片表面粗糙度Ra值为0.281nm,表面光滑,划痕等表面微观缺陷明显改善。

【Abstract】 With advanced electro-manufacture developing so fast,glass substrate as a kind of widely used material in the mechanical manufacture is forced to be ultra-smooth.Nano-sized CeO2 was prepared by sol-gel method and characterized by X-ray diffraction and TOF-SIMS.It shows that the average particle diameter is 13.3nm and particle size distribution is uniform.The polishing performances of nano-sized CeO2 on glass substrate were studied.ZYGO profiler indicated that the average roughness(Ra) of the surface was reduced to about 0.6nm.Atom Force Microscopy(AFM) showed that a super smooth surface with Ra of 0.281nm was obtained within 5μm×5μm area and micro-defects such as micro-scratches can hardly be observed.

【基金】 国家自然科学基金(50575131);上海市纳米专项资助项目(0452nm013)
  • 【分类号】TB383.1
  • 【被引频次】57
  • 【下载频次】1059
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