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铽-N-苯基邻氨基苯甲酸的合成及荧光性质
Synthesis of Rare Earth Complexes with N-Phenylanthranilic Acid and its Fluorescence Property
【摘要】 采用共沉淀法制备了稀土铽的N-苯基邻氨基苯甲酸二元配合物。同时,采用溶胶-凝胶法制备了掺杂稀土铽的N-苯基邻氨基苯甲酸二元配合物的SiO2凝胶玻璃复合发光体,研究了合成的2种配合物的热稳定性及荧光性质。结果表明,在凝胶玻璃中合成的稀土二元配合物,其热稳定性明显提高,而其特征荧光基本保持不变。
【Abstract】 Binary complex of rare earth(Tb) with N-phenylanthranilic acid was synthesized by homogenous precipitation method.In addition,the complex was synthesized by sol-gel method in the gel glass.The thermal decomposition and fluorescence spectra for the gel phosphors were measured.Compared with solid powder complex sample,the thermal stability of this complex was enhanced in SiO2 host matrix and the fluorescence spectra remained unchanged.
【基金】 湛江师范学院重点科研项目资助
- 【文献出处】 化工技术与开发 ,Technology & Development of Chemical Industry , 编辑部邮箱 ,2006年12期
- 【分类号】O641.4
- 【下载频次】133