Synthesis and Crystal Structure of 5-N-i-Propyl-2-(2′-nitrobenzenesulfonyl)-glutamine

【Abstract】 The title compound, 5Ni%propyl2(2′nitrobenzenesulfonyl)glutamine, was synthesized and its structure was confirmed by IR, MS, {}~1H NMR, and elemental analysis. The single crystal structure of the title compound was determined by Xray diffraction. The crystal belongs to Monoclinic, space group %P%2(1), with a=0.69281(11) nm, b=0.76508(12), c=1.5843(3) nm, α=90°, β=90.941(3)°, γ=90°, V=0.8397(2) nm~3, Z=2, D-c=1.477 g/cm~3, μ=0.236 mm~ -1 , F(000)=392, R=0.0297, and wR=0.0664.更多还原