节点文献
毛细管电泳高频电导法测定几种中药中的丁香酚
Determination of Eugenol in Several Chinese Herbal Medicines by Capillary Electrophoresis with High Frequency Conductivity Method
【Abstract】 A method based on capillary electrophoresis with a high frequency conductivity method was(developed) for the determination of eugenol in several Chinese herbal medicines from different producing areas.In this study,some key factors for separation and detection were studied and the best analysis conditions were obtained.In the buffer system of 2.0 mmol/L triethylamine +0.74 mol/L methanol at separation potential of 18.0 kV,the optimal separation and detection was obtained.Under the chosen conditions,eugenol was eluted within 7 min.The linear range of eugenol was 2.0—540 μg/mL,the limit of detection was 0.6 μg/mL,and the recovery ranged from 93.3% to 106%.
【关键词】 毛细管电泳;
高频电导检测;
非接触式电导检测;
丁香酚;
中草药;
【Key words】 Capillary electrophoresis; High frequency conductivity detection; Contactless conductivity detection; Eugenol; Chinese herbal medicine;
【Key words】 Capillary electrophoresis; High frequency conductivity detection; Contactless conductivity detection; Eugenol; Chinese herbal medicine;
【基金】 国家自然科学基金(批准号:20375049);广东省自然科学基金重点项目(批准号:021808)资助
- 【文献出处】 高等学校化学学报 ,Chemical Journal of Chinese Universities , 编辑部邮箱 ,2006年11期
- 【分类号】R284
- 【被引频次】18
- 【下载频次】224