节点文献
藏药麻花艽中四种苦苷类化学成分的HPLC测定
Determination of four iridoid glycosides in tibetan medicine Gentiana straminea Maxim.by HPLC
【摘要】 建立了藏药麻花艽中龙胆苦苷(gentiopicroside)、落干酸(loganic acid)、獐牙菜苦苷(swertiamarin)和獐牙菜苷(sweroside)4种苦苷类成分的HPLC分析方法。色谱柱为Eclipse XDB-C8(4.6 mm i.d.×150 mm,5μm),流动相为体积分数5%乙腈+10 mmoL甲酸~95%乙腈水溶液,检测波长为240 nm。结果表明,该方法具有良好的线性关系和回收率,为麻花艽中苦苷类成分的进一步开发利用提供了科学依据。
【Abstract】 The contents of four iridoids(gentiopicroside,loganic acid,swertiamarin,sweroside) in Gentiana straminea were determined by high performance liquid chromatography(HPLC).The analysis was performed on Eclipse XDB-C8(4.6 mm i.d.×150 mm,5 μm) column,eluted with the solution of 0.01 mol/L methanoic acid with 5% acetonitrile and 95% acetonitrile and with UV detection at 240 nm.All calibration curves indicated good linear regression(r≥0.9999) within test ranges.
【关键词】 藏药;
麻花艽;
龙胆苦苷;
落干酸;
獐牙菜苦苷;
獐牙菜苷;
HPLC;
【Key words】 Tibetan medicine; Gentiana straminea Maxim.; Gentiopicroside; Loganic acid; Swertiamarin sweroside; HPLC;
【Key words】 Tibetan medicine; Gentiana straminea Maxim.; Gentiopicroside; Loganic acid; Swertiamarin sweroside; HPLC;
【基金】 国家中西部专项项目(2001BA901A47);中国科学院知识创新工程领域前沿项目(CXLY-2002-08)资助
- 【文献出处】 分析试验室 ,Chinese Journal of Analysis Laboratory , 编辑部邮箱 ,2006年05期
- 【分类号】R29
- 【被引频次】31
- 【下载频次】289