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高效液相色谱法快速测定水中的苯并(a)芘
Rapid Determination of Benzopyrene in Water by high performance liquid chromatography
【摘要】 本文建立了一种水中苯并(a)芘的快速测定方法。以环己烷萃取,过滤,浓缩,定容,用反相HPLC测定,方法的检出限为0.0025μg/L,RSD(n=8)为2.9%,加标回收率为98.9%—106.9%。
【Abstract】 A rapid method for the determination of benzopyrene was developed.Sample was extracted with cyclohexane,filtrate?concentrate?fixed cubage and then determined by reversed-phase HPLC.The detection limit was 0.0025μg/L.The relative standard deviation (n=8) was2.9%.The recoveries are in the range of 98.9%-106.9.
- 【文献出处】 福建分析测试 ,Fujian Analysis & Testing , 编辑部邮箱 ,2006年01期
- 【分类号】X832
- 【被引频次】3
- 【下载频次】178