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医用NiTi合金表面双层生物活性薄膜的制备及表征
Preparation and characterization of bilayer bioactive film on medical NiTi alloy surface
【摘要】 采用溶胶-凝胶法在NiTi合金基体上制备出TiO2-SiO2-HAP梯度生物活性薄膜,通过仿生合成进一步制备了TiO2-SiO2-HAP/HAP双层生物活性薄膜。SEM、XRD和FTIR对复合薄膜的测试结果表明,外层的HAP薄膜呈多孔网状;电化学腐蚀测试表明,与TiO2-SiO2-HAP梯度生物活性薄膜相比,TiO2-SiO2-HAP/HAP双层生物活性薄膜的抗腐蚀性进一步增强。
【Abstract】 This paper reports the preparation of TiO2-SiO2-HAP/HAP bilayer bioactive film on NiTi alloy substrate by Sol-Gel method.It is formed on the basis of TiO2-SiO2-HAP gradient bioactive film through biomimetic synthesis process.Characterization by SEM、XRD and FTIR demonstrates that the outer HAP appears porous and net structure.Electro-chemical measurement reveals that the corrosion resistance of TiO2-SiO2-HAP/HAP bilayer bioactive film is better than that of the TiO2-SiO2-HAP gradient bioactive film.
【关键词】 梯度生物活性薄膜;
仿生合成;
溶胶凝胶法;
NiTi合金;
抗腐蚀性;
【Key words】 gradient bioactive film; biomimetic synthesis; Sol-Gel method; NiTi alloy; the corrosion resistance;
【Key words】 gradient bioactive film; biomimetic synthesis; Sol-Gel method; NiTi alloy; the corrosion resistance;
【基金】 辽宁省教育厅A类攻关项目(202073425);辽宁省博士启动基金项目(20021054)
- 【文献出处】 大连轻工业学院学报 ,Journal of Dalian Institute of Light Industry , 编辑部邮箱 ,2006年03期
- 【分类号】R318.08
- 【被引频次】4
- 【下载频次】124