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离子交换富集-原子吸收光谱法测定单矿物中的锰
Atomic Absorption Spectrometry Determination of Trace Manganese in Mineral by Separation and Pro-concentration with ion exchange process
【摘要】 采用了离子交换分离富集矿样中的锰,该系统与原子吸收测量技术相结合,实现了富集-原子吸收法联用测定矿样中的锰,,该方法检出限(3σ)为0.018μg/L,线性范围0.01~0.5μg/L,相对标准偏差RSD为3.59%。该法应用于标准样品的测定其结果与标准样值相符,应用于实际矿样的测定,加标回收率在96.7%~104.3%之间,结果满意。
【Abstract】 A rapid and sensitive method for concentration and separation of trace manganese based on ion exchange process has been developed.The detection limit of the method is 0.018μg/L.The recoveries are in the range of 96.7% to 104.3% and The relative standard deviations(RSD)are 3.59%.The method has been successfully applied for the determination of manganese in certified reference material GBW07268 and other sample.
【关键词】 离子交换分离富集;
原子吸收光谱法;
测定;
锰;
【Key words】 Ion exchange process; Separation and Pro-concentration; AAS; Manganese;
【Key words】 Ion exchange process; Separation and Pro-concentration; AAS; Manganese;
- 【文献出处】 东北电力大学学报 ,Journal of Northeast Dianli University , 编辑部邮箱 ,2006年01期
- 【分类号】P575.4
- 【被引频次】1
- 【下载频次】70