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Nd:YAG激光陶瓷纳米粉体的制备方法研究
Fabricating of Nanometer Powders for Nd:YAG Ceramic Laser Materials
【摘要】 本文采用共沉淀法和溶胶-凝胶法成功合成了1at.%和5at.%的Nd:YAG纳米粉体,并采用TG-DTA、XRD及SEM对前驱体粉体进行表征,最后采用真空热压烧结工艺制得Nd:YAG多晶陶瓷,并对陶瓷晶粒进行了形貌分析.根据实验结果,找出了获得多晶陶瓷的较优配方和影响Nd:YAG陶瓷材料透光度的因素.
【Abstract】 In this work, 1at.% and 5at.%Nd:YAG nano-meter powders were obtained in chemical co-precipitation method and sol-gel method. And the Nd:YAG precursor powders were characterized by TG-DTA、XRD and SEM. At last, polycrystal Nd:YAG powders were sintered under vacuum atmosphere for cermics, in addition, ceramics grains were represented by SEM. Finally, it has found out that the optimum method of fabricating polycrystal Nd:YAG ceramics, and factors influencing on optical transmittance of Nd:YAG ceramics laser materials.
【关键词】 Nd:YAG陶瓷;
前驱体粉末;
共沉淀法;
溶胶-凝胶法;
【Key words】 Nd:YAG ceramics; precursor powder; co-precipitation method; sol-gel method;
【Key words】 Nd:YAG ceramics; precursor powder; co-precipitation method; sol-gel method;
【基金】 陕西省攻关项目-添加剂梯度分布特殊结构Nd:YAG激光陶瓷的研究资助(2005k06-G11)
- 【文献出处】 传感技术学报 ,Chinese Journal of Sensors and Actuators , 编辑部邮箱 ,2006年05期
- 【分类号】TQ174.1
- 【被引频次】3
- 【下载频次】440