【摘要】 以氨基磺酸为催化剂,通过环己酮和1,2-丙二醇反应合成了环己酮1,2-丙二醇缩酮。实验表明,在酮醇物质的量比为1∶1.2,催化剂用量为2%,环己烷15mL,反应时间80min的条件下,环己酮1,2-丙二醇缩酮的收率可达99.2%。更多还原

【Abstract】 Cyclohexanone 1,2-propanediol ketal was synthesized from cyclohexanone and 1,2-propanediol using sulfamic acid as catalyst. The optimum conditions are: molar ratio of cyclohexanone to 1,2-propanediol was 1:1.2,the amount of catalyst was 2.0%,the reaction time was 80 min and its yield can reach up 99.2%.更多还原