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大孔树脂对栀子苷分离效果的研究
Effect of macroporous resin in separation of gardenoside
【摘要】 目的 优选分离栀子苷的大孔树脂。方法 将栀子粗提液置大孔树脂中吸附 ,并以水、70 %乙醇分别洗脱 ,以 HPL C法测定洗脱液中栀子苷含量。结果 D30 1R、D396、D2 96和 AB- 8四种型号大孔树脂效果差异较大。结论 D30 1R型大孔树脂用作栀子苷的分离效果较好。
【Abstract】 Object To optimize the macroporous resin for separating gardenoside. Methods Putting the extract fluid of Gardenia jasmincides Ellis into pillar was adsorbed with macroporous resin, then washed by water, 70% alcohol in succession to determine the content of gardenoside by HPLC. Results D301R, D396, D296, and AB-8, the four macroporous resins’ effects were different a lot. Conclusion D301R macroporous resin is effective to separate the gardenoside.
【基金】 国家中医药管理局中医药科学技术研究基金资助项目 (国中医药科 0 0 -0 1KZ0 1号 )
- 【文献出处】 中草药 ,Chinese Traditional and Herbal Drugs , 编辑部邮箱 ,2002年09期
- 【分类号】R284.2
- 【被引频次】67
- 【下载频次】654