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丁酸正戊酯的催化合成
Catalytic synthesis of pentyl butyrate
【摘要】 以硫酸氢钠为催化剂 ,正本酸与正戊醇为原料合成了丁酸正戊酯。最佳合成条件 :以 0 1mol正丁酸为基准 ,醇酸摩尔比 1 3,催化剂用量 1 0g ,反应时间 1 0h ,酯收率达 88 3%。该催化剂具有价廉易得 ,催化活性好 ,反应时间短 ,使用方便等优点。
【Abstract】 Pentyl butyrate was synthesized by reaction of n butyric acid and n pentanol with sodium bisulfate as catalyst.The optimum conditions for the reaction were the followings:basing on 0 1mol n butyric acid,molar ratio of n pentanol to n butyric acid was 1 3,mass of catalyst was 1 0g,and reaction time was 1 0 hr.The yield of pentyl butyrate was up to 88 3% under these conditions.Sodium bisulfate catalyst is low cost,high active and convenient in preparation and use.
- 【文献出处】 天然气化工 ,Natural Gas Chemical Industry , 编辑部邮箱 ,2002年05期
- 【分类号】O623.624
- 【被引频次】1
- 【下载频次】49