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野甘菊中小白菊内酯的超临界流体色谱测定

DETERMINATION OF PARTHENOLIDE IN FEVERFEW USING SUPERCRITICAL FLUID CHROMATOGRAPHY

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【作者】 郭亚东吴双凤李璠

【Author】 GUO Ya-dong,WU Shuang-feng,LI Fan (Department of Pharmacy,Kunming Medical College,Kunming 650031,China)

【机构】 昆明医学院药学院昆明医学院药学院 昆明650031昆明650031昆明650031

【摘要】 用超临界流体色谱法分析野甘菊中小白菊内酯时 ,具有很好的精密度和线性关系 ,其保留时间和峰面积的相对标准偏差分别为 2 6 7%和 0 70 % ,相关系数为 0 9996。样品经甲醇提取后直接进样分析 ,并在 3min内完成 ,可用于快速检测

【Abstract】 Determination of parthenolide in feverfew by SFC was studied in this paper.The precision and linearity of the detector response were excellent,the RSD were 2.67% and 0.70% respectively for retention time and peak area,the value of correlation coeffcient(r 2)was 0.9996.The sample was determined directly after it was extracted with CH 3OH,and it was finished within 3 minutes.This method could be used to analyse parthenolide in feverfew rapidly.

【关键词】 超临界流体色谱野甘菊小白菊内酯
【Key words】 SFCParthenolideFeverfew
  • 【文献出处】 天然产物研究与开发 ,Natural Product Research and Development , 编辑部邮箱 ,2002年02期
  • 【分类号】O657.7
  • 【被引频次】19
  • 【下载频次】341
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