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奶油甘油三酯的毛细管气相色谱-EI质谱分析

Determination of Composition of Triacylglycerols in Butterfat by Capillary Gas Chromatography-EI Mass Spectrometry

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【作者】 邹建凯

【Author】 ZOU Jian-kai(Department of Chemistry, School of Science, Zhejiang University, Hangzhou 310027, China)

【机构】 浙江大学理学院化学系 浙江杭州310027

【摘要】 以HP5MS30m×0.25mm×0.25μm毛细管柱分离奶油中各甘油三酯 ,通过各自EI质谱确定其组成 ,共鉴定出108种甘油三酯 ,其中以丁酸双棕榈酸三甘油酯 (8.2% ,峰面积百分比 ,下同 )、癸酸双棕榈酸三甘油酯 (7.9% )、月桂酸双棕榈酸三甘油酯 (7.7% )、肉豆蔻酸双棕榈酸三甘油酯 (6.9% )、丁酸棕榈酸油酸三甘油酯 (6.2% )、丁酸棕榈酸硬脂酸三甘油酯 (5.9% )为主

【Abstract】 A method for analyzing the composition of triacylglycerols in butterfat was developed by high temperature gas chromatography-electron impact mass spectrometry with HP-5 MS 30 m×0.25 mm×0.25 μm capillary column. According to the analysis of GC-MS, 108 triacylglycerols were identified. The main triacylglycerols include butyrodipalmitin, dipalmitocaprin, dipalmitolaurin, dipalmitomyristin, butyropalmito-olein and butyropalmitostearin with relative contents of 8.2%, 7.9%, 7.7%, 6.9%, 6.2% and 5.9%, respectively.

  • 【文献出处】 分析测试学报 ,Journal of Instrumental Analysis , 编辑部邮箱 ,2002年05期
  • 【分类号】O657.63
  • 【被引频次】7
  • 【下载频次】191
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