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仿生溶液法诱导钛表面形成钙磷涂层的研究

Preparation of Calcium Phosphate Coatings on Surfaces of Commercially Pure Titanium Induced by Simulated Body fluid

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【作者】 邓炜王贻宁蒋滔陈群周彬程祥荣

【Author】 Deng Wei △ Wang Yining Jiang Tao Chen Qun Zhou Bin Cheng Xiangrong (Department of Prosthodontics, College & Hospital of Stomatology, Wuhan University,Wuhan 430079)

【机构】 武汉大学口腔医学院修复科武汉大学口腔医学院修复科 武汉430079现在江西省赣南医学院附属医院口腔科武汉430079武汉4

【摘要】 采用 3种不同的方法即不作处理、酸和碱处理但不加热、酸和碱处理后 6 0 0℃加热对商用纯钛进行表面处理 ,然后将样品浸泡于仿生溶液中 2周后 ,经过处理的两组样品表面均形成一层薄的钙磷涂层。 SEM和 EDX分析表明 :酸碱处理再经 6 0 0℃加热组较单纯的酸碱处理组涂层晶体构型均一 ;XRD分析表明晶体组成主要为含有少量氯元素的羟基磷灰石

【Abstract】 All samples were divided into three groups and subjected to three different surface treatments, i.e. untreated group, group etched with mixed acid of 1:1 HCl and H 2SO 4 followed by immersion in 6N NaOH solution at 60℃ for 24h and group etched with mixed acid of 1:1 HCl and H 2SO 4 followed by immersion in 6N NaOH solution at 60℃ for 24h then heated at 600℃ for 1h. After soaked in simulated body fluid for two weeks, a thin calcium phosphate coatings was precipitated on the surfaces of the two treated samples. Results of SEM and EDX showed that calcium phosphate coatings on the surfaces of the titanium samples etched and heated were more even than the titanium samples etched without heating. The analysis of XRD demonstrated the main component of calcium phosphate coating was hydroxyapatite.

【基金】 国家自然科学基金资助项目 ( 39970 80 0 )
  • 【文献出处】 生物医学工程学杂志 ,Journal of Biomedical Engineering , 编辑部邮箱 ,2002年03期
  • 【分类号】R783.1
  • 【被引频次】27
  • 【下载频次】202
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