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正交试验法优选仙鹤草中总黄酮的提取工艺
EXTRACTION TECHNOLOGY OF TOTAL FLAVONOIDS IN AGRIMONIA PILOSA
【摘要】 采用正交试验法研究仙鹤草中总黄酮的提取工艺 ,考察了浸提液浓度、浸提温度、浸提时间、浸提次数、液料比等 5个因素对仙鹤草总黄酮含量的影响。确立了仙鹤草总黄酮最佳提取条件为 :浸提液体积分数4 0 % ,液料比 10∶1,浸提温度 70℃ ,回流提取 3次 ,每次 0 .5h。
【Abstract】 Extraction technology of flavonoids in Agrimonia pilosa was studied by orthogonal experiment.Effects of ethanol water solvent,extraction temperature,extraction time,extraction times and ratio of liquid to material on flavonoid content were investigated.Optimum extraction condition was determined as follows:volume parts of the composition of ethanol water solvent 40%,ratio of liquor to material 10 ∶1,three times of reflux extraction at 70 ℃,each for 0.5 h.
- 【文献出处】 林产化学与工业 ,Chemistry & Industry of Forest Products , 编辑部邮箱 ,2002年03期
- 【分类号】TQ461
- 【被引频次】27
- 【下载频次】376