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硼酸酯化法合成聚乙二醇(6000)单硬脂酸酯

Synthesis of Polyethylene Glycol (6000) Monostearate by Method of Boric Acid Esterification

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【作者】 陈红;

【Author】 Chen Hong ( Chemical Engineering Department of Liaoyang Petrochemical College, Liaoyang 111003)

【机构】 辽阳石油化工高等专科学校化工系 辽阳 111003;

【摘要】 采用硼酸酯化法合成了聚乙二醇(6000)单硬脂酸酯,试验考察了反应时间、反应温度、催化剂用量、物料比等对产物中聚乙二醇(6000)单硬脂酸酯含量的影响,确定了最佳合成条件。在此条件下,产物中聚乙二醇(6000)单硬脂酸酯的含量可达93%。

【Abstract】 Polyethylene glycol(6000) monostearate was prepared from polyethylene glycol(6000) and boric acid by esterification. The effects of reaction time, reaction temperature, catalyst amount, and molar ratio of materials on the content of polyethylene glycol(6000) monostearate in the product were investigated. The optimum synthesis condition was determined. The content of polyethylene glycol(6000) monostearate in the product could reach 93% under the optimum condition.

  • 【文献出处】 精细石油化工进展 ,Advances in Fine Fetrochemicals , 编辑部邮箱 ,2002年06期
  • 【分类号】TQ423
  • 【被引频次】8
  • 【下载频次】561
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